Publications


PublicationPDF
Regio- and Stereo-Selective Isomerization of Borylated 1,3-Dienes Enabled by Selective Energy Transfer Catalysis, Byeongseok Kweon, Lukas Blank, Julia Soika, Amélia Messara, Constantin Daniliuc, Ryan Gilmour, 2024, ttps:/doi.org/10.1002anie.202404233
Addressing Reproducibility Challenges in High-Throughput Photochemistry Brenda Pijper, Lucía M. Saavedra, Matteo Lanzi, Maialen Alonso, Alberto Fontana, Marta Serrano, José Enrique Gómez, Arjan W. Kleij, Jesús Alcázar, Santiago Cañellas, ChemRxic, 2024, 10.26434/chemrxiv-2024-n12vr
Synthesis of polysubstituted azepanes by dearomative ring expansion of nitroarenes, Rory Mykura, Raquel Sánchez-Bento, Esteban Matador, Vincent K. Duong, Ana Varela, Lucrezia Angelini, Rodrigo J. Carbajo , Josep Llaveria , Alessandro Ruffoni , & Daniele Leonori , Nat. Chem., 2024, ttps:/doi.org/10.1038s41557-023-01429-1
Metal-free Photocatalytic Cross-Electrophile Coupling enables C1 Homologation and Alkylation of Carboxylic Acids with Aldehydes Stefano Bonciolini,† Antonio Pulcinella,† Matteo Leone, Debora Schiroli, Adrián Luguera Ruiz, Andrea Sorato, Maryne A. J. Dubois, Ranganath Gopalakrishnan, Geraldine Masson, Nicola Della Ca’, Stefano Protti, Maurizio Fagnoni, Eli Zysman-Colman, Magnus Johansson, and Timothy Noël,* ChemRxiv, 2023, 10.26434/chemrxiv-2023-fcl2j-
Automated self-optimization, intensification, and scale-up of photocatalysis in flow, Aidan Slattery†, Zhenghui Wen†, Pauline Tenblad†, Jesús Sanjosé-Orduna, Diego Pintossi,Tim den Hartog, Timothy Noël*, Science, 2024. https:/doi.org/10.1126science.adj1817-
Adrián Luguera Ruiz, Elena Mariani, Stefano Protti and Maurizio Fagnoni , Photoredox catalyzed release of carbon-based radicals from 2-substituted-1,3-imidazolidines, 2024, https:/doi.org/10.1039D3QO01856C-
Raquel Sa´nchez-Bento, Baptiste Roure, Josep Llaveria, Alessandro Ruffoni and Daniele Leonori, A strategy for ortho-phenylenediamine synthesis via dearomative-rearomative coupling of nitrobenzenes and amines, Chem (2023), https:/doi.org/10.1016j.chempr.2023.10.008-
Damiano Diprima, Hannes Gemoets, Stefano Bonciolini and Koen Van Aken*, Selective and scalable oxygenation of heteroatoms using the elements of nature: air, water, and light, Beilstein J. Org. Chem. 2023, 19, 1146–1154. https:/doi.org/10.3762bjoc.19.82-
Brenda Pijper, Raúl Martín, Alberto J. Huertas-Alonso, Maria Lourdes Linares, Enol López, Josep Llaveria, Ángel Díaz-Ortiz, Darren J. Dixon, Antonio de la Hoz,* and Jesús Alcázar, Fully Automated Flow Protocol for C(sp3 )−C(sp3 ) Bond Formation from Tertiary Amides and Alkyl Halides, April 27, 2023, https:/doi.org/10.1021acs.orglett.3c01390-
Aidan Slattery, Zhenghui Wen, Pauline Tenblad, Diego Pintossi, Jesus Sanjose-Orduna, Tim den Hartog, Timothy Noel. An all-in-one multipurpose robotic platform for the self-optimization, intensification and scale-up of photocatalysis in flow, ChemRxiv, 2023, 10.26434/chemrxiv-2023-r0drq-
Max Wienhold, Byeongseok Kweon, Calum McLaughlin, Matthias Schmitz, Till Zähringer, Constantin G. Daniliuc, Christoph Kerzig, and Ryan Gilmour. Geometric Isomerisation of Bifunctional Vinyl Fluoride Linchpins: Stereodivergence in Amide and Polyene Bioisostere Synthesis. Angew. Chem. Int. Ed. 2023, e202304150. https:/doi.org/10.1002anie.202304150-
Gabriela Oksdath-Mansilla, Fabricio Roman Bisogno, Brenda Pijper, Jesus Alcazar. Challenge and opportunity: The two edges of continuous-flow photochemistry. Chem Catalysis 3, 100487, January 19, 2023 https:/doi.org/10.1016j.checat.2022.100487 -
Brenda Pijper, Jesus Alcazar, Gabriela Oksdath-MansillaFabricio, Roman Bisogno. Continuous-flow photochemistry as an automated platform integrated with closed-loop AI/ML approaches. Chem Catalysis 3, 100488, January 19, 2023 https:/doi.org/10.1016j.checat.2022.100488-
Brenda Pijper, Irini Abdiaj, Daniele Leonori, and Jesus Alcázar, Development of an automated platform for C(sp3)-C(sp3) bond formation via XAT chemistry, ChemCatChem, 2023,15, e2022012 https:/doi.org/10.1002cctc.202201289-
Irini Abdiaj, Santiago Cañellas, Alejandro Dieguez, Maria Lourdes Linares, Brenda Pijper, Alberto Fontana, Raquel Rodriguez, Andres Trabanco, Eduardo Palao, and Jesus Alcázar End-to-End Automated Synthesis of C(sp3)-Enriched Drug-like Molecules via Negishi Coupling and Novel, Automated Liquid–Liquid Extraction J. Med. Chem., 2022, 66, 1, 716–732 https:/doi.org/10.1021acs.jmedchem.2c01646-
Antonio Pulcinella, Stefano Bonciolini, Florian Lukas, Andrea Sorato, Timothy Noel, Photocatalytic Alkylation of C(sp3)−H Bonds Using Sulfonylhydrazones, Angew. Chem. Int. Ed.2022, e202215374 https:/doi.org/10.1002anie.202215374-
Luca Capaldo, Stefano Bonciolini, Antonio Pulcinella, Manuel Nuno and Timothy Noel , Modular allylation of C(sp3)–H bonds by combining decatungstate photocatalysis and HWE olefination in flow† Chem. Sci., 2022, 13, 7325 DOI: 10.1039/d2sc01581a-
Emanuele Pinosa, Elena Bassan, Sultan Cetin, Marco Villa, Simone Potenti, Francesco Calogero, Andrea Gualandi, Andrea Fermi*, Paola Ceroni, and Pier Giorgio Cozzi, Light-Induced Access to Carbazole-1,3-dicarbonitrile: A Thermally Activated Delayed Fluorescent (TADF) Photocatalyst for Cobalt-Mediated Allylations, J. Org. Chem, 2021 https:/doi.org/10.1021acs.joc.2c01825-
Megan Amy Bryden, Francis Millward, Tomas Matulaitis, Dongyang Chen, Marco Villa, Andrea Fermi, Sultan Cetin, Paola Ceroni, and Eli Zysman-Colman, Moving Beyond Cyanoarene Thermally Activated Delayed Fluorescence Compounds as Photocatalysts: An Assessment of the Performance of a Pyrimidyl Sulfone Photocatalyst in Comparison to 4CzIPN. J. Org. Chem., 2022 https:/doi.org/10.1021acs.joc.2c01137-
Adrián Luguera Ruiz , Marta La Mantia, Daniele Merli, Stefano Protti, and Maurizio Fagnoni, Alkyl Radical Generation via C–C Bond Cleavage in 2-Substituted Oxazolidines, ACS Catal. 2022, 12, 19, 12469–12476 https:/doi.org/10.1021acscatal.2c03768
Stefano Bonciolini, Timothy Noël and Luca Capaldo Synthetic Applications of Photocatalyzed Halogen-radical mediated Hydrogen Atom Transfer for C−H Bond Functionalization. European Journal of Organic Chemistry 2022, DOI: https:/doi.org/10.1002ejoc.202200417
Jiyaun Lyu, Matteo Leone, Aurélie Claraz, Clémence Allain, Luc Neuville and Géraldine Masson. Syntheses of new chiral chimeric photo-organocatalysts, RSC Adv., 2021,11, 36663-36669 DOI https:/doi.org/10.1039D1RA06885G